Three solvents, three flowsheets
A processor chooses hydrocarbon for terpene-rich concentrates, ethanol for throughput and distillate, or supercritical CO2 for a solvent-free label, and each comes with a different set of exchangers. Hydrocarbon lines chill propane and butane to -40 to -80 F and recover the solvent on a chilled condenser. Ethanol lines chill, evaporate and condense. CO2 lines run the solvent through a heater into the vessel and through a separator and a condenser back to the pump at 1,000 to 5,000 psi.
Post-processing is common to all three: winterization, decarboxylation at 220 to 250 F, and distillation with a condenser on the vapor. The ethanol flowsheet in detail is on the CBD Extraction page.
Butane boils at 31 F and propane at -44 F, so a hydrocarbon line stores the solvent under its own vapor pressure and chills it to -40 to -80 F before injection to keep terpenes and leave waxes. The chiller is a shell-and-tube on a low-temperature fluid at -90 F, rated for the solvent's vapor pressure at the warmest temperature it could see, about 175 psig for propane at 100 F. After extraction the solvent is boiled off the extract in a jacketed collection vessel at 90 to 100 F and the vapor goes to a recovery condenser, a shell-and-tube with hydrocarbon in the tubes and chilled fluid at 0 to 20 F on the shell, which liquefies it back to the solvent tank. The condenser sets the recovery rate; an undersized one turns a 30 minute recovery into two hours.
Supercritical CO2 runs at 1,500 to 5,000 psi and 90 to 120 F through the biomass, drops pressure in one or more separators where the extract falls out, and returns the CO2 to a condenser at 40 to 60 F and 600 to 900 psi for the pump. The exchangers are a preheater ahead of the vessel, cooling on the separators to control what drops out, and the recycle condenser. Every one is a pressure vessel first: a coil-in-shell or small shell-and-tube rated well above 5,000 psi on the CO2 side, ASME stamped, in 316L. The duties are small and the design is about pressure, not cleanability.
Decarboxylation heats crude to 220 to 250 F for an hour or more in a jacketed reactor on hot oil or 60 psig steam, with a small condenser on the vent that catches terpenes and water driven off. Distillation, wiped-film or short-path, runs at 300 to 400 F under deep vacuum with an internal condenser fed by a circulating heater-chiller. The external condensers on these steps are small vertical shell-and-tube units on tower or tempered water, sized on the vapor rate the reactor vendor states with a generous sub-cooling section, because a decarb condenser that lets terpene vapor past it makes the room smell and loses product.
Hydrocarbon extraction is done in a Class I Division 1 room and ethanol in Class I Division 2. A heat exchanger has no electrical parts, but the skid, transmitters, valves and chiller are classified, and the exchanger is specified with them in mind: no elastomer that ethanol or butane swells, no aluminum in a propane line, clamps rated for the pressure, and full drainability so solvent does not sit in a shell after shutdown. The common mistake is a plate exchanger on a hydrocarbon duty: the gasket seam is a leak path for flammable gas under pressure and most jurisdictions will not accept it. Hydrocarbon exchangers are welded shell-and-tube.
Send the solvent, the recovery rate, the vessel ratings, the chiller fluid and the room classification and HeatX quotes the set.
Call and talk it through with an engineer: 1-805-484-2992
The solvent sets the build, so each row is read by solvent: hydrocarbon, ethanol or CO2. Find yours, compare it with your room classification and send both with the quote request.
| Condition | Detail |
| Product | Propane and butane blends; ethanol; CO2 at supercritical conditions; crude and distillate downstream |
| Flow range | Hydrocarbon recovery 20 to 200 lb/h; ethanol 5 to 60 gpm; CO2 10 to 100 lb/min |
| Temperatures in / out | Hydrocarbon chilled to -40 to -80 F, recovered at 90 to 100 F; CO2 heated to 90 to 120 F, condensed at 40 to 60 F |
| Hold | Vessel residence 5 to 30 minutes; decarb 60 to 90 minutes at 220 to 250 F |
| Utility | Low-temperature fluid to -90 F for hydrocarbon chillers; chilled water for CO2 condensers; hot oil or steam for decarb |
| Approach | 10 to 15 F on cryogenic chillers; 5 to 10 F on CO2 condensers; 20 F on decarb heaters |
| Construction | Shell-and-tube for hydrocarbon at pressure; plate for ethanol; coil or shell-and-tube rated 5,000 psi for CO2 |
| Finish / class | 316L product side, 32 Ra; food-grade gaskets; pressure rating per the solvent, ASME stamp on hydrocarbon and CO2 vessels |
| Area classification | C1D1 for hydrocarbon rooms, C1D2 for ethanol, unclassified for CO2 |
| CIP | Solvent flush between runs; periodic hot ethanol or caustic clean |
Above the solvent vapor pressure at the warmest temperature the equipment could ever reach, not the temperature it normally runs. Propane is 175 psig at 100 F and about 225 psig at 120 F, which a shell left in the sun or a condenser with the chiller off can see, so 250 psig is the usual minimum design pressure on propane service and the relief valve is set at or below it and sized for the fire case. Butane is only about 37 psig at 100 F, which is why a condenser bought for butane and later run on a propane-heavy blend ends up rated below its contents. State the heaviest propane fraction the line will ever run on the inquiry and the rating follows from it.
Yes, as part of the technical report most codes now require for the whole extraction system. The International Fire Code chapter on plant extraction and NFPA 1 both call for a licensed engineer's report on the equiptment before the room is approved, and the exchangers are listed in it with the rest of the pressure equipment. The reviewer looks for the ASME data report, design pressure and temperature, the relief device and its set pressure, and the wetted material list for each unit. A report that stalls on one missing data report holds up the entire permit, so ask for the stamped data report and the material list with the quote, not after delivery.
With a relief device on every section that can be blocked in, on both sides of the tube wall. Liquid CO2 trapped between two closed valves and warmed toward room temperature passes its critical point at 88 F and 1,071 psia, and the pressure of a liquid-full system climbs steeply past that, so each isolable section gets its own relief. The utility side is the case skids miss: a tube failure in a CO2 heater or condenser puts CO2 at 600 to 5,000 psi into a water or glycol shell rated for 150, so the shell carries a rupture disk sized for a full tube break or is rated for the CO2 side. Relief lines are kept short and warm, because CO2 expanding below 75 psia forms dry ice that can block them.
Aluminum, brass and any elastomer the solvent swells or that cannot survive rapid depressurization. On propane and butane the gaskets are PTFE or a fluoroelastomer; EPDM and natural rubber swell in hydrocarbons within hours. On ethanol EPDM is acceptible. On CO2 the problem is different: elastomers absorb CO2 at 1,500 psi and above and blow apart from the inside when the pressure is dropped quickly, so O-rings and gaskets are chosen for explosive decompression resistance and the system is depressurized slowly. Brass stays out wherever the extract continues to food or supplement use because of its lead content.
Yes, through how fully it condenses, how far it sub-cools and how completely it drains. Terpenes boil well above 300 F and mostly stay in the collection vessel, but a condenser that floods or holds pockets of liquid lets light terpenes and water accumulate in the returned solvent run after run, and the next strain inherits the last one's aroma. A condenser with the chilled fluid at 0 to 20 F, a vent at the top for non-condensables and a drain at the true bottom returns clean liquid to the tank.
Mostly by the CO2 itself, which sweeps the separators and condenser on every run. The separator coolers and the surfaces downstream of them are where extract collects, and where a site changes between products with distinct profiles those are rinsed with ethanol and dried before the next run. That is why the CO2 exchangers on this page are 316L and drainable even though the duties are small and the design is about pressure: a coil or bundle that holds a pocket of extract cannot be shown clean. Ask for drain points at the true low point of every CO2 exchanger on the drawing.
Cold ethanol in, crude out, solvent back to the tank: the four exchangers on a hemp line and how each is sized
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Jacket water at 37 C, held to a tenth of a degree, by a heater and a cooler that never touch the culture.
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Below -20 F the fluid on the cold side is the design, and the exchanger is sized on it, not on the solvent.
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